第一部分 绪论Part One Introduction
一、物理化学实验的目的和要求
二、物理化学实验的安全知识
三、物理化学实验的设计思想
四、误差理论和有效数字
五、实验数据的表示法和处理
1.Objective and requirement
2.Physical chemistry laboratory safety
3.Rules for designing of the physical chemistry experiment
4.Error theory and significant figures
5.Data reporting
第二部分 实验Part Two Experjments
实验一 燃烧热的测定
Experiment 1 Heats Of Combustion
实验二 溶解热的测定
Expenment 2 Heats of Solution
实验三 凝固点降低法测定摩尔质量和渗透压
Experiment 3 Molar Mass and Osmotic:Pressure by Freezing Point
Depression
实验四 液体饱和蒸气压的测定
Expenment 4 Saturated Vapor Pressure of Pure LJquids
实验五 反应平衡常数及分配系数的测定
Expenment 5 Equilibrium Constant 0f Reaction and PaItitiml
Coefficient
实验六 完全互溶双液系平衡相图的绘制
Expenment 6 Phase Diagram of a Miscible Binary Liquid Svstem
实验七 双组分简单低共熔体系相图的绘制
Expenment 7 Solid-liquid Binary Phase Diagram
实验八 三组分液-液系统相图的绘制
Experiment 8 A Ternary Phase Diagram for a System of Three
Liquids
实验九 电解质水溶液电导的测定及应用
Experiment 9 Measurement and Application of Electrolyte Solution
Conductance
实验十 电动势法测溶液pH和反应热力学函数
Experiment 10 Determinations of pH of Solution and Thermodynamic
Functions
by Electromotive Force Measurements
实验十一 一级反应速率常数的测定
Experiment 11 Rate Constant for First Order Reaction
实验十二 碘化钾与过氧化氢反应的速率常数及活化能的测定
Experiment 12 Kinetics of Reaction between Potassium Iodide and
Hydrogen
Peroxide
实验十三 丙酮溴化反应速率常数的测定
Experiment 13 Rate Constant and Activation Energy of the
Bromination of
Acetone
实验十四 乙酸乙酯皂化反应速率常数及活化能的测定
Experiment 14 Rate Constant for the Saponification of Ethyl
Acetate by
Conductometric Method
实验十五 最大泡压法测定溶液的表面张力
Experiment 15 Surface Tension of Solutions by Bubble Pressure
Method
实验十六 固体在溶液中的吸附
Experiment 16 Adsorption of Solids in Solution
实验十七 乳状液的制备和性质
Experiment 17 Preparation and Properties of Emulsion
实验十八 溶胶的制备及性质
Experiment 18 Preparation and Properties of Sols
实验十九 黏度法测定大分子的平均相对分子质量
Experiment 19 Average Relative Molar Mass of the Macromolecule by
Viscosity Method
实验二十 纳米材料的合成与表征综合设计性试验
Experiment 20 Preparation and Characterization of Nanomaterials
Multi—designing Experiment
实验二十一 药物稳定性及有效期测定设计性实验
Experiment 21 Determination of Drug Stability and Shelf Life
Designing Experiment
实验二十二 固体药物常规理化常数的测定综合设计性实验
Experiment 22 Physical and Chemical Constants of Drugs
Multi—designing Experiment
附录Appendices
常用物理化学数据表Reference Data of Experimental Physical Chemistry
参考文献References